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When serendipity knocks on the door: Synthesis and Physicochemical Characterization of 7-Chloro-2,3-dihydro-5H-thiazolo[3,2-a]pyrimidin-5-one 

Carmona-Vargas, Christian C.; Ellena, Javier; D’Vries, Richard F.; Chaur, Manuel N. (Sociedade Brasileira de Quimica, 2019-03-19)
Herein, we present the serendipitous obtaining of 7-chloro-2,3-dihydro-5H-thiazolo [3,2-a]pyrimidin-5-one in 40% yield by using POCl3 and a thiobarbituric acid derivative. The thiazolopyrimidine derivative was characterized ...
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Mechanochemical Synthesis of a Multicomponent Solid Form: The Case of 5-Fluorocytosine Isoniazid Codrug 

Souza, Matheus S.; Diniz, Luan F.; Vogt, Lautaro; Carvalho Jr., Paulo S.; D’vries, Richard F.; Ellena, Javier (American Chemical Society, 2018-07-12)
Mechanochemistry synthesis was applied to the supramolecular synthesis and green scale-up production of a 1:1 drug–drug cocrystal involving the antimetabolite prodrug 5-Fluorocytosine (5-FC) and the tuberculostatic drug ...
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Avoiding irreversible 5-fluorocytosine hydration: Via supramolecular synthesis of pharmaceutical cocrystals 

Souza, Matheus S.; Diniz, Luan F.; Vogt, Lautaro; Carvalho, Paulo S. Jr.; D’vries, Richard F.; Ellena, Javier (Royal Society of Chemistry, 2018-07-27)
The antimetabolite 5-fluorocytosine (5-FC) was used to form pharmaceutical cocrystals in order to modulate its poor physicochemical stability in humid environments, which leads to the irreversible incorporation of a water ...
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Spergulagenic Acid A: Isolation and single crystal structure elucidation 

Montoya, Guillermo; Gutierrez, Gustavo; D'vries Arturo, Richard Fernando; Ellena, Javier; Panay, Aram J. (Elsevier B.V., 2019-07-19)
In the present work, the crystal structure of (3b)-3-acetoxy-30-methoxy-30-oxo-olean-12-en-28-oic acid, (Spergulagenic Acid A) is presented. The compound was isolated from Cecropia telenitida roots, employing semi-pilot ...
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1D lanthanide coordination polymers based on lanthanides and 4′-hydroxi-4-biphenylcarboxylic acid: Synthesis, structures and luminescence properties 

D'vries Arturo, Richard Fernando; Gomez, German E.; Mondragon, Lina Paola; Onna, Diego; Barja, Beatriz C.; Soler-Illia, Galo J.A.A.; Ellena, Javier (Academic Press Inc., 2019-03-29)
Synopsis: A family of coordination polymers with formula [Ln(4-OHBBA) 3 (H 2 O) 2 ] with a new 3D supramolecular network topology was obtained. Luminescence properties were studied. Resume: A new family of 1D coordination ...
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Novel Isoniazid cocrystals with aromatic carboxylic acids: Crystal engineering, spectroscopy and thermochemical investigations 

Diniz, Luan F.; Souza, Matheus S.; Carvalho Jr, Paulo S.; da Silva, Cecilia C.P.; D'vries Arturo, Richard Fernando; Ellena, Javier (Elsevier B.V., 2017-09-30)
Four novel cocrystals of the anti-tuberculosis drug Isoniazid (INH), including two polymorphs, with the aromatic carboxylic acids p-nitrobenzoic (PNBA), p-cyanobenzoic (PCNBA) and p-aminobenzoic (PABA) were rationally ...
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Data of synthesis, characterization and luminescence measurements in 1D lanthanide coordination polymers based on lanthanides 

D'vries Arturo, Richard Fernando; Gomez, German E.; Mondragon, Lina Paola; Onna, Diego; Barja, Beatriz C.; Soler-Illia, Galo J.A.A.; Ellena, Javier (Elsevier Inc., 2019-10-22)
In this work are presented all the conditions of synthesis explored to obtain a new family of compound with formula [Ln(4-OHBBA)3(H2O)2] (Ln = La, Pr). Powder X ray diffraction was used to identify the different phases ...
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Order-disorder phase transition induced by proton transfer in a co-crystal of 2,4-dichlorobenzoic acid and trimethylamine: N -oxide 

D'vries Arturo, Richard Fernando; Moreno Fuquen, Rodolfo; Camps, Ihosvany; Ayala, Alejandro Pedro; Kennedy, Alan R.; Reinheimer, Eric W.; Ellena, Javier (Royal Society of Chemistry, 2017-06-05)
A crystalline binary adduct between trimethylamine N-oxide (TMANO) and 2,4-dichlorobenzoic acid (2,4-DCBA) molecules was obtained by slow evaporation from acetonitrile. The obtained molecular complex is formed by a racemic ...

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Ellena, Javier (8)
D'vries Arturo, Richard Fernando (5)Diniz, Luan F. (3)Souza, Matheus S. (3)Barja, Beatriz C. (2)D’vries, Richard F. (2)Gomez, German E. (2)Mondragon, Lina Paola (2)Onna, Diego (2)Soler-Illia, Galo J.A.A. (2)... View MoreSubjectCoordination polymers (2)Hydrogen bonds (2)Lanthanide metals (2)Luminescence (2)Supramolecular topology (2)4 aminobenzoic acid (1)Atoms (1)Bioactivity (1)Caffeine (1)Chlorination (1)... View MoreDate Issued2019 (4)2017 (2)2018 (2)Has File(s)
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